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Methods for the sampling and analysis of lead and lead alloys -- Sulphur in lead and lead alloys
This Part of BS 3908 describes a method for the determination of the amount of sulphur present in lead and lead alloys by titrimetry.
It is applicable to sulphur contents in the range 0.0001 % to 0.02 % by mass.
NOTE The titles of the publications referred to in this standard are listed on the inside back cover.
Method for the determination of **sulphur** within the range *0.0001% to 0.02%* by mass.
The sample is reacted with acid and the *hydrogen sulphide evolved* is absorbed in sodium hydroxide-methanol mixture, which is then titrated with mercury (II) acetate.
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